Influence of solid-phase and melt synthesis methods on the structure and electrochemical properties of Na3Fe2(PO4)3 polycrystals

A. S. Nogai, Artur A. NOGAI, D. E. Uskenbaev, E. A. Nogai, Alexander A. BUSH

Kimyo va kimyo texnologiyasi · 2024-yil

Annotatsiya

The article studies the influence of solid-phase and melt synthesis methods on the structure and electrochemical properties of the Na3Fe2(PO4)3 polycrystals. If the solid-phase synthesis of the Na3Fe2(PO4)3 polycrystals (type 1 of samples) is carried out using ceramic technology, initially glassy precursors are first obtained by melting the starting materials under the influence of optical radiation energy at the melt synthesis method, and the Na3Fe2(PO4)3 polycrystals are obtained after firing (type 2 of samples). With this method, the synthesis of polycrystals occurs quickly under sharp temperature-gradient conditions, therefore, the monoclinic distortions of α-Na3Fe2(PO4)3 structure are partially removed under the influence of compressive deformation. Due to the greater symmetrization of the α-Na3Fe2(PO4)3 crystal structure and the higher density of type 2 samples, their electrochemical properties are improved. As a result of a comparative assessment of the structures and electrochemical properties of the Na3Fe2(PO4)3 polycrystals, it was shown that samples of the second type have better cutting and higher densities and energy capacities than samples of the first type.

Maqola ma’lumotlari
MualliflarA. S. Nogai, Artur A. NOGAI, D. E. Uskenbaev, E. A. Nogai, Alexander A. BUSH
JurnalKimyo va kimyo texnologiyasi
NashriyotТошкент кимё-технология институти
ISSN1992-9498, 2181-1121
Nashr sanasi2024-07-03
Jild2024
Son2
TilIngliz
Ilmiy sohaKimyo
DOI10.70189/1992-9498.1619
Indeksga qo‘shilgan2026-09-02

Ilmiy soha

Iqtibos keltirish

APAA. S. Nogai, Artur A. NOGAI, D. E. Uskenbaev, E. A. Nogai, & Alexander A. BUSH (2024). INFLUENCE OF SOLID-PHASE AND MELT SYNTHESIS METHODS ON THE STRUCTURE AND ELECTROCHEMICAL PROPERTIES OF Na3Fe2(PO4)3 POLYCRYSTALS. Kimyo va kimyo texnologiyasi, 2024(2). https://doi.org/10.70189/1992-9498.1619
GOST (OAK)A. S. Nogai va b. INFLUENCE OF SOLID-PHASE AND MELT SYNTHESIS METHODS ON THE STRUCTURE AND ELECTROCHEMICAL PROPERTIES OF Na3Fe2(PO4)3 POLYCRYSTALS // Kimyo va kimyo texnologiyasi. – 2024. – T. 2024, № 2. – DOI: 10.70189/1992-9498.1619.
MLAA. S. Nogai, Artur A. NOGAI, D. E. Uskenbaev, E. A. Nogai, and Alexander A. BUSH. “INFLUENCE OF SOLID-PHASE AND MELT SYNTHESIS METHODS ON THE STRUCTURE AND ELECTROCHEMICAL PROPERTIES OF Na3Fe2(PO4)3 POLYCRYSTALS.” Kimyo va kimyo texnologiyasi, 2024(2), 2024. https://doi.org/10.70189/1992-9498.1619
ChicagoA. S. Nogai, Artur A. NOGAI, D. E. Uskenbaev, E. A. Nogai, and Alexander A. BUSH. “INFLUENCE OF SOLID-PHASE AND MELT SYNTHESIS METHODS ON THE STRUCTURE AND ELECTROCHEMICAL PROPERTIES OF Na3Fe2(PO4)3 POLYCRYSTALS.” Kimyo va kimyo texnologiyasi, 2024(2) (2024). https://doi.org/10.70189/1992-9498.1619
HarvardA. S. Nogai, Artur A. NOGAI, D. E. Uskenbaev, E. A. Nogai, and Alexander A. BUSH (2024) ‘INFLUENCE OF SOLID-PHASE AND MELT SYNTHESIS METHODS ON THE STRUCTURE AND ELECTROCHEMICAL PROPERTIES OF Na3Fe2(PO4)3 POLYCRYSTALS’, Kimyo va kimyo texnologiyasi, 2024(2). https://doi.org/10.70189/1992-9498.1619
BibTeX
@article{asnogai2024,
  title = {INFLUENCE OF SOLID-PHASE AND MELT SYNTHESIS METHODS ON THE STRUCTURE AND ELECTROCHEMICAL PROPERTIES OF Na3Fe2(PO4)3 POLYCRYSTALS},
  author = {A. S. Nogai and Artur A. NOGAI and D. E. Uskenbaev and E. A. Nogai and Alexander A. BUSH},
  journal = {Kimyo va kimyo texnologiyasi},
  year = {2024},
  volume = {2024},
  number = {2},
  doi = {10.70189/1992-9498.1619},
  url = {https://doi.org/10.70189/1992-9498.1619}
}

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