Synthesis of thiocol oligomer based on sodium tetrasulphide, epichlorhydrine and ammonium phosphate

NORMURODOV, Bakhtiyor, TURAEV, Khayit, JALILOV, Abdulakhat, KASIMOV, Sherzod

Kimyo va kimyo texnologiyasi · 2021-yil

Annotatsiya

The aim is to synthesize and study thiokol oligomer NEP-12 based on sodium tetrasulfide, epichlorohydrin and ammonium phosphate, which is intended for use as the main component of thiokol sealant. To achieve this goal, a thiokol oligomer based on sodium tetrasulfide, epichlorohydrin, and ammonium phosphate has been synthesized and investigated, and the optimal conditions for the synthesis of a thiokol oligomer have been determined. Research has been carried out on the influence of the molar ratios of the starting substances on the composition and physicochemical properties of the synthesized thiocol oligomer. 80 °C was taken as the optimum polycondensation temperature, the reaction time in this case is 1.5-2 hours, as a result, the yield of the target product reaches 94%. The thiokol oligomer with the best performance was obtained at a 1: 1: 1 molar ratio of sodium tetrasulfide, epichlorohydrin, and ammonium phosphate, respectively. Based on the results of IR spectroscopy and differential scanning calorimetry, a reaction for the formation of a thiokol oligomer is proposed.

Maqola ma’lumotlari
MualliflarNORMURODOV, Bakhtiyor, TURAEV, Khayit, JALILOV, Abdulakhat, KASIMOV, Sherzod
JurnalKimyo va kimyo texnologiyasi
NashriyotТошкент кимё-технология институти
ISSN1992-9498, 2181-1121
Nashr sanasi2021-04-25
Betlar32-37
TilIngliz
Ilmiy sohaKimyo
DOI10.51348/sulj4315
Indeksga qo‘shilgan2026-09-02

DOI: 10.51348/sulj4315 · Maqolaning asl sahifasi

Ilmiy soha

Kimyo

Iqtibos keltirish

APANORMURODOV, Bakhtiyor, TURAEV, Khayit, JALILOV, Abdulakhat, & KASIMOV, Sherzod (2021). Synthesis of thiocol oligomer based on sodium tetrasulphide, epichlorhydrine and ammonium phosphate. Kimyo va kimyo texnologiyasi, 32-37. https://doi.org/10.51348/sulj4315
GOST (OAK)NORMURODOV, Bakhtiyor va b. Synthesis of thiocol oligomer based on sodium tetrasulphide, epichlorhydrine and ammonium phosphate // Kimyo va kimyo texnologiyasi. – 2021. – P. 32-37. – DOI: 10.51348/sulj4315.
MLANORMURODOV, Bakhtiyor, TURAEV, Khayit, JALILOV, Abdulakhat, and KASIMOV, Sherzod. “Synthesis of thiocol oligomer based on sodium tetrasulphide, epichlorhydrine and ammonium phosphate.” Kimyo va kimyo texnologiyasi, 32-37, 2021. https://doi.org/10.51348/sulj4315
ChicagoNORMURODOV, Bakhtiyor, TURAEV, Khayit, JALILOV, Abdulakhat, and KASIMOV, Sherzod. “Synthesis of thiocol oligomer based on sodium tetrasulphide, epichlorhydrine and ammonium phosphate.” Kimyo va kimyo texnologiyasi, 32-37 (2021). https://doi.org/10.51348/sulj4315
HarvardNORMURODOV, Bakhtiyor, TURAEV, Khayit, JALILOV, Abdulakhat, and KASIMOV, Sherzod (2021) ‘Synthesis of thiocol oligomer based on sodium tetrasulphide, epichlorhydrine and ammonium phosphate’, Kimyo va kimyo texnologiyasi, 32-37. https://doi.org/10.51348/sulj4315
BibTeX
@article{normurodovbakhtiyor2021,
  title = {Synthesis of thiocol oligomer based on sodium tetrasulphide, epichlorhydrine and ammonium phosphate},
  author = {NORMURODOV, Bakhtiyor and TURAEV, Khayit and JALILOV, Abdulakhat and KASIMOV, Sherzod},
  journal = {Kimyo va kimyo texnologiyasi},
  year = {2021},
  pages = {32-37},
  doi = {10.51348/sulj4315},
  url = {https://doi.org/10.51348/sulj4315}
}

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